I followed instructions in the silica TMOS recipe from http://www.aerogel.org and successfully produced some small pieces of aerogel in my home shop.
The two main difficulties are: 1. Getting TMOS or TEOS (the key chemical ingredient), and 2. Building a supercritical drying chamber. The components for the chamber can be bought from http://www.mcmaster.com or another source of industrial pipe fittings. You’ll also need a supply of liquid carbon dioxide. I used a 20-lbs cylinder, which I bought from a local welding store. Most of the cost is in the cylinder itself, since a refill costs only $20 to $30. You may find a welding supply shop that will rent the cylinder.
Getting the TMOS is difficult since chemical suppliers are generally unwilling to sell to individuals…
Make a robot friend with Adafruit’s CRICKIT – A Creative Robotics & Interactive Construction Kit. It’s an add-on to our popular Circuit Playground Express, FEATHER and other platforms to make and program robots with CircuitPython, MakeCode, and Arduino. Start controlling motors, servos, solenoids. You also get signal pins, capacitive touch sensors, a NeoPixel driver and amplified speaker output. It complements & extends your boards so you can still use all the goodies on the microcontroller, now you have a robotics playground as well.